By Garcia J.L.L., de Castro M.D.L.
This ebook goals to supply scientists with information regarding a chain of strategies that may be used so as to facilitating the transformation of the pattern to a suitable nation for next detection or quantitation of its parts of curiosity. The thoughts handled variety from the extremely simple ones (e.g. freeze-drying) to different extra complicated ones (e.g. glow discharge and laser-induced breakdown sampling).
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Extra info for Acceleration And Automation Of Solid Sample Treatment
It is therefore essential to ensure that the product temperature is maintained within such limits during the sublimation step. One way to ascertain that the sublimation step has completed is by monitoring the pressure rise in the drying chamber as a result of temporarily isolating it from the pumping system . An increase in chamber pressure at a given shelf pressure will result in an increase in product temperature. Such a temperature increase may exceed the collapse temperature and result in collapse or, under extreme conditions, in meltback of the product.
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